No, but he came close. From CNN:

Michael Jackson died while preparing to set a world record for the most successful concert run, but he unknowingly set another record that led to his death. Jackson may be the only human ever to go two months without REM—rapid eye movement—sleep, which is vital to keep the brain and body alive. The 60 nights of propofol infusions Dr. Conrad Murray said he gave Jackson to treat his insomnia is something a sleep expert says no one had ever undergone.

Also:

If the singer had not died on June 25, 2009, of an overdose of the surgical anesthetic, the lack of REM sleep may have taken his life within days anyway, according to [Harvard Medical School sleep expert Dr. Charles] Czeisler's testimony Friday. Lab rats die after five weeks of getting no REM sleep, he said. It was never tried on a human until Murray gave Jackson nightly propofol infusions for two months. Translating that to a human, Czeisler estimated, Jackson would have died before his 80th day of propofol infusions. Murray told police he had given it to him for 60 nights before trying to wean him off it on June 22, 2009—three days before his death.

Michael Jackson will never not be fascinating.